# Introduction  (Page 3/3)

 Page 3 / 3

## Results:

You should observe a gas bubbling up into the second test tube. This reaction happens quite rapidly.

## Conclusions:

When hydrogen peroxide is added to manganese dioxide it decomposes to form oxygen and water. The chemical decomposition reaction that takes place can be written as follows:
$2{\mathrm{H}}_{2}{\mathrm{O}}_{2}\to 2\mathrm{H}{}_{2}\mathrm{O}+{\mathrm{O}}_{2}$
Note that the manganese dioxide is a catalyst and is not shown in the reaction. (A catalyst helps speed up a chemical reaction.)

The previous experiment used the downward displacement of water to collect a gas. This is a very common way to collect a gas in chemistry. The oxygen that is evolved in this reaction moves along the delivery tube and then collects in the top of the test tube. It does this because it is lighter than water and so displaces the water downwards. If you use a test tube with an outlet attached, you could collect the oxygen into jars and store it for use in other experiments.

The above experiment can be very vigourous and produce a lot of oxygen very rapidly. For this reason you use dilute hydrogen peroxide and only a small amount of manganese dioxide.

## Synthesis reactions

During a synthesis reaction , a new product is formed from elements or smaller compounds. The generalised equation for a synthesis reaction is as follows:

$\mathrm{A}+\mathrm{B}\to \mathrm{AB}$

One example of a synthesis reaction is the burning of magnesium in oxygen to form magnesium oxide( [link] ). The equation for the reaction is:

$2\mathrm{Mg}+{\mathrm{O}}_{2}\to 2\mathrm{MgO}$

## Aim:

To demonstrate the synthesis of iron sulphide from iron and sulphur.

## Apparatus:

5,6 g iron filings and 3,2 g powdered sulphur; porcelain dish; test tube; Bunsen burner

## Method:

1. Measure the quantity of iron and sulphur that you need and mix them in a porcelain dish.
2. Take some of this mixture and place it in the test tube. The test tube should be about 1/3 full.
3. This reaction should ideally take place in a fume cupboard. Heat the test tube containing the mixture over the Bunsen burner. Increase the heat if no reaction takes place. Once the reaction begins, you will need to remove the test tube from the flame. Record your observations.
4. Wait for the product to cool before breaking the test tube with a hammer. Make sure that the test tube is rolled in paper before you do this, otherwise the glass will shatter everywhere and you may be hurt.
5. What does the product look like? Does it look anything like the original reactants? Does it have any of the properties of the reactants (e.g. the magnetism of iron)?

When working with a bunsen burner work in a well ventilated space and ensure that there are no flammable substances close by. Always tuck loose clothing in and ensure that long hair is tied back.

## Results:

1. After you removed the test tube from the flame, the mixture glowed a bright red colour. The reaction is exothermic and produces energy .
2. The product, iron sulphide, is a dark colour and does not share any of the properties of the original reactants. It is an entirely new product.

## Conclusions:

A synthesis reaction has taken place. The equation for the reaction is:
$\mathrm{Fe}+\mathrm{S}\to \mathrm{FeS}$

## Apparatus:

Bunsen burner, 4 test tubes, a test tube rack and a test tube holder, small spatula, pipette, magnet, a birthday candle, $\mathrm{NaCl}$ (table salt), $0,1\phantom{\rule{2pt}{0ex}}\mathrm{M}\phantom{\rule{4pt}{0ex}}{\mathrm{AgNO}}_{3}$ , $6\phantom{\rule{2pt}{0ex}}\mathrm{M}\phantom{\rule{4pt}{0ex}}\mathrm{HCl}$ , magnesium ribbon, iron filings, sulphur.

${\mathrm{AgNO}}_{3}$ stains the skin. Be careful when working with it or use gloves.

## Method:

1. Place a small amount of wax from a birthday candle into a test tube and heat it over the bunsen burner until it melts. Leave it to cool.
2. Add a small spatula of $\mathrm{NaCl}$ to 5 ml water in a test tube and shake. Then use the pipette to add 10 drops of ${\mathrm{AgNO}}_{3}$ to the sodium chloride solution. NOTE: Please be careful ${\mathrm{AgNO}}_{3}$ causes bad stains!!
3. Take a 5 cm piece of magnesium ribbon and tear it into 1 cm pieces. Place two of these pieces into a test tube and add a few drops of $6\phantom{\rule{2pt}{0ex}}\mathrm{M}\phantom{\rule{4pt}{0ex}}\mathrm{HCl}$ . NOTE: Be very careful when you handle this acid because it can cause major burns.
4. Take about 0,5 g iron filings and 0,5 g sulphur. Test each substance with a magnet. Mix the two samples in a test tube and run a magnet alongside the outside of the test tube.
5. Now heat the test tube that contains the iron and sulphur. What changes do you see? What happens now, if you run a magnet along the outside of the test tube?
6. In each of the above cases, record your observations.

## Questions:

Decide whether each of the following changes are physical or chemical and give a reason for your answer in each case. Record your answers in the table below:
 Description Physical or chemical change Reason melting candle wax dissolving $\mathrm{NaCl}$ mixing $\mathrm{NaCl}$ with ${\mathrm{AgNO}}_{3}$ tearing magnesium ribbon adding $\mathrm{HCl}$ to magnesium ribbon mixing iron and sulphur heating iron and sulphur

#### Questions & Answers

are nano particles real
yeah
Joseph
Hello, if I study Physics teacher in bachelor, can I study Nanotechnology in master?
no can't
Lohitha
where we get a research paper on Nano chemistry....?
nanopartical of organic/inorganic / physical chemistry , pdf / thesis / review
Ali
what are the products of Nano chemistry?
There are lots of products of nano chemistry... Like nano coatings.....carbon fiber.. And lots of others..
learn
Even nanotechnology is pretty much all about chemistry... Its the chemistry on quantum or atomic level
learn
da
no nanotechnology is also a part of physics and maths it requires angle formulas and some pressure regarding concepts
Bhagvanji
hey
Giriraj
Preparation and Applications of Nanomaterial for Drug Delivery
revolt
da
Application of nanotechnology in medicine
has a lot of application modern world
Kamaluddeen
yes
narayan
what is variations in raman spectra for nanomaterials
ya I also want to know the raman spectra
Bhagvanji
I only see partial conversation and what's the question here!
what about nanotechnology for water purification
please someone correct me if I'm wrong but I think one can use nanoparticles, specially silver nanoparticles for water treatment.
Damian
yes that's correct
Professor
I think
Professor
Nasa has use it in the 60's, copper as water purification in the moon travel.
Alexandre
nanocopper obvius
Alexandre
what is the stm
is there industrial application of fullrenes. What is the method to prepare fullrene on large scale.?
Rafiq
industrial application...? mmm I think on the medical side as drug carrier, but you should go deeper on your research, I may be wrong
Damian
How we are making nano material?
what is a peer
What is meant by 'nano scale'?
What is STMs full form?
LITNING
scanning tunneling microscope
Sahil
how nano science is used for hydrophobicity
Santosh
Do u think that Graphene and Fullrene fiber can be used to make Air Plane body structure the lightest and strongest. Rafiq
Rafiq
what is differents between GO and RGO?
Mahi
what is simplest way to understand the applications of nano robots used to detect the cancer affected cell of human body.? How this robot is carried to required site of body cell.? what will be the carrier material and how can be detected that correct delivery of drug is done Rafiq
Rafiq
if virus is killing to make ARTIFICIAL DNA OF GRAPHENE FOR KILLED THE VIRUS .THIS IS OUR ASSUMPTION
Anam
analytical skills graphene is prepared to kill any type viruses .
Anam
Any one who tell me about Preparation and application of Nanomaterial for drug Delivery
Hafiz
what is Nano technology ?
write examples of Nano molecule?
Bob
The nanotechnology is as new science, to scale nanometric
brayan
nanotechnology is the study, desing, synthesis, manipulation and application of materials and functional systems through control of matter at nanoscale
Damian
Is there any normative that regulates the use of silver nanoparticles?
what king of growth are you checking .?
Renato
Richard is sitting on his chair and reading a newspaper three (3) meters away from the door
The fundamental frequency of a sonometer wire streached by a load of relative density 's'are n¹ and n² when the load is in air and completly immersed in water respectively then the lation n²/na is
Properties of longitudinal waves