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Chem217labsfall07

OpenStax
@
  Diels-alder and melting point
0.1 Experiment 1: diels-alder and melting point
0.2 Background information
0.3 Part 1: melting point
0.4 Part 2: diels-alder reaction
0.5 Mechanism
0.6 Some important facts
0.7 Stereochemistry of d.a. reaction
0.8 Grading
0.9 Experimental procedure for melting point
0.10 Part i. the effect of purity on melting point
0.11 2. once the two pure melting points have been determined find a partner
0.12 Part ii. determination of an unknown substance
0.13 Experimental procedure for diels-alder
0.14 Part iii. diels alder reaction
0.15   Waste disposal
0.16 Approximate lab time 2-2.5 hours
0.17 Part 2: melting point (total 10 points)
1   Aldol condensation
2   Grignard reaction
3   Friedel-crafts reaction

Source:  OpenStax, Chem217labsfall07. OpenStax CNX. Oct 16, 2007 Download for free at http://cnx.org/content/col10463/1.4
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